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Notes from the loop

Why thermal interface materials pump out

Grease fails at the bond line, not at the die.


The paste sits where it was squeezed at assembly. Under thermal cycling it migrates outward until the interface is starved, and the joint runs hotter at the same power.

Gradual failure · found by a trend line, not by an alarm

Grease, minimum interface 0.05mm
Phase-change transition 45–55°C

Ask for the specification sheet

Die-cut thermal pad lying on a cold-plate surface with its release liner partly lifted, photographed close

Bond line · die-cut pad on a cold plate

01 / The failure

The same joint, drawn at one scale

Assembly on the left, after cycling on the right.

At assembly After cycling clamp load starved centre paste fills the bond line paste at the perimeter Lid Cold plate Lid Cold plate 0.05 mm bond line

Bond line · assembly and after cycling · one scale

02 / The mechanism

Two bodies, one interface, different expansion

The interface sits between a package or lid and a cold plate. Different coefficients of thermal expansion move the two bodies against each other on every power cycle. The grease absorbs that movement, and it is the layer that gets pumped.

Grease 0.05 Phase change 0.20–1.0 Gap pad 0.5–6 Custom pad to 20 0.05 0.2 1 5 20 mm

Bond line by material class

The dimension that decides the failure is the bond line.
Interface Figure Set by
Thermal grease 0.05 mm minimum clamp load
Phase-change sheet 0.20 to 1.0 mm supplied thickness
Gap pad 0.5 to 6 mm supplied thickness
Custom pad to 20 mm drawing
Bond line the dominant term assembly pressure

Assembly pressure belongs in the failure analysis, not in the installation notes.

Dry contact Filled under 3 % of the area contact resistance cut by more than 90 %   Air gap remains Material wets both faces

Contact asperities · dry and filled

03 / Why the interface dominates

Dry metal touches on a fraction of its area

Two apparently flat surfaces in dry contact touch on less than 3 % of their apparent area. The interface resistance that air-filled contact creates is what a thermal material is bought to remove, and filling the interface is credited with cutting contact resistance by more than 90 %.

Interface resistance below 0.05 °C·cm²/W

Commercial phase-change sheet at ≤0.0078 °C·cm²/W over 0.20–1.0 mm, ASTM D5470

Chip reliability is estimated to fall by 5 % for every 1 °C rise in operating temperature in the 70–80 °C band. Pump-out buys that rise slowly and charges for it at the end.

04 / Dry-out

Dry-out and pump-out are fixed by different things

Grease also loses carrier fluid at temperature, which hardens the paste and raises interface resistance even where the bond line survives.

The published proxy: thermal weight loss

Below 0.2 % after 48 hours at 125 °C, with dry-out resistance declared to a 150 °C ceiling.

A proxy, not a lifetime. It is the only dry-out figure most datasheets carry.

Dry-out ceiling by material class.
Class Ceiling Proxy
Thermal grease 150 °C thermal weight loss
Phase-change sheet 125 °C thermal weight loss
Silicone pad 125 °C thermal weight loss
125 150 °C 0.4 0.2 0 % 0.2 % phase change grease

Weight loss against soak temperature

05 / Silicone bleed

The compliance question behind a materials detail

Free silicone oil migrates out of a pad or a grease, coats contact surfaces and can reach the coolant loop. A European buyer asking for a low-siloxane or silicone-free thermal material is answering a compliance question rather than expressing a preference.

Oil bleed

1 % or less, on a 30 mm filter paper disc at 25 % compression, 125 °C, for 48 hours.

REACH SVHC candidate list

Past 240 substances, and it includes the silicones D4, D5 and D6.

Low-siloxane claim

Published as a D3–D20 figure. One pad is below 20 ppm, with outgassing at TML 0.170 % and CVCM 0.010 % by ASTM E595.

06 / Phase change
Phase-change sheet laid on a cold plate with its backing partly peeled back and the edge thickness of the sheet visible
Phase-change sheet

A sheet that softens in place

A phase-change sheet is solid at room temperature and softens in service, wetting the surfaces at a transition a running loop reaches anyway: 45 to 55 °C by ASTM D3418. It stays in the gap, closing the pump-out path.

8.5 W/m·K through-plane · 0.20–1.0 mm · ≤0.0078 °C·cm²/W by ASTM D5470, test pressure not published · ≥3.0 kV/mm · −40 to +125 °C · UL 94 V-0

The cost is assembly discipline: the pad stays below its transition until the joint is closed.

The codes behind this post

Ask for another code
  • EMS-TM-PC85 Phase-change sheet 45–55 °C by ASTM D3418 PDF
  • EMS-TM-G35 Thermal grease 0.020 °C·in²/W at 30 psi PDF
  • EMS-TM-P50-20 Gap filler pad 2.0 mm · impedance at 10, 30 and 50 psi PDF
  • EMS-TM-GR120 Graphene pad 0.50–6.0 mm · through-plane only PDF
07 / Cured pad

The second countermeasure

The pad trades a little thermal performance for a bond line that cannot migrate.

Through-plane unless stated.
Property Grease Phase change Cured pad
Bond line under cycling pumped outward held in the gap cannot migrate
Impedance, with its condition 0.020 °C·in²/W at 30 psi 0.0078 °C·cm²/W 0.154–0.539 at 10 psi; 0.061–0.129 at 50 psi
Thickness 0.05 mm minimum 0.20–1.0 mm 0.5–5 mm · 32 Shore 00
Its failure mode starved centre dry-out delamination
10 50 psi 0.6 0.4 0.2 0 °C·in²/W 5 mm 0.5 mm endpoints published

Impedance against pressure

Two variants matter at a warped plate: an ultra-soft pad at 1.2 W/m·K over 1.0 mm and 10 Shore 00, at 10, 30 and 50 psi, and a high-rebound oriented pad at 70 % rebound.

Adhesive area trades assembly convenience against interface resistance: more glue points hold the pad better and conduct worse.

08 / The measurement

A conductivity figure with no pressure and no thickness is not a specification

ASTM D5470 returns apparent thermal impedance at a controlled pressure and thickness. Conductivity is derived by measuring impedance at several thicknesses and regressing: the intercept is contact resistance and the slope gives the conductivity.

through-plane in-plane cold plate lid

Measurement directions on one pad

A 2× difference in conductivity does not produce a 2× difference in impedance at the same bond line. Send the gap, the assembly pressure and the target impedance rather than a conductivity target.

Oriented pads also carry an in-plane figure, measured along the plane rather than across it. It is a different measurement, and it does not share a column with any through-plane figure on this page.

Through-plane · across the thickness · the figure every table here carries

09 / Specification sheet

Ask for the specification sheet

Leave your email and the model code. The specification sheet, the drawing and the datasheet for the code come back within one working day.

Specification request

Ask for the specification sheet

Leave your work email and the model code. One datasheet per model, with position resolution and locating repeatability stated as separate rows.

  • A specification table of at least ten rows per product family, and a downloadable PDF for every model listed.
  • Seal-life data where it decides the choice: permeation rate, compression set and fluid compatibility.
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